氧氮?dú)浞治鰞x的常見(jiàn)故障及解決方法:氧和氮空白值超過(guò)20。這是由于氣流小,不能將爐子中的空氣驅(qū)趕出去。可調(diào)節(jié)氣體流量,調(diào)節(jié)載氣壓力在0.2~0.4MPa。接通儀器載氣,放一個(gè)石墨坩堝在下電極上,打開(kāi)主電源開(kāi)關(guān),點(diǎn)擊軟件上的關(guān)爐按鈕,關(guān)閉爐子并等待10s。調(diào)節(jié)流量調(diào)節(jié)器,直到流量計(jì)a顯示為30L/h,打開(kāi)爐子。調(diào)節(jié)調(diào)節(jié)器直到流量計(jì)b顯示為50L/h,再次關(guān)閉爐子。如果以上設(shè)置不穩(wěn)定,則增加流量至100L/h,反復(fù)調(diào)節(jié)直至儀器穩(wěn)定。分析儀,就選上海禹重實(shí)業(yè)有限公司,歡迎客戶來(lái)電!安徽力可氧氮?dú)浞治鰞x咨詢報(bào)價(jià)Instrumentcalibration/driftcorrection.a.Loginam...
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SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbefor
User-FriendlyBrandSoftwareCornerstoneLECOsexclusivebrandsoftwareenablestheusertohavecompleteaccesstoanalysisCornerstonecontrol,methodsettings,diagnostics,reporting,andmoreinahighlyorganizedandimmersiveenvironment.Designedthroughacollaborationofcustomerfeedbackandinnovativeengineering,Cornerstoneallo
SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedi
Instrumentcalibration/driftcorrectionf.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.g.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.h.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanal
Instrumentcalibration/driftcorrectionf.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.g.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.h.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanal
氧氮?dú)浞治鰞x的使用注意事項(xiàng):1、氧氮?dú)浞治鰞x在初次啟用前,應(yīng)該對(duì)連接點(diǎn)、焊點(diǎn)、閥門(mén)等進(jìn)行檢漏,以確??諝庵械难醪粫?huì)反滲進(jìn)入管道及儀器內(nèi)部,造成測(cè)量數(shù)值偏高。2、再次使用儀器前,要進(jìn)行管道系統(tǒng)凈化,將漏入的空氣除干凈,同時(shí)確保連接取樣管路時(shí)沒(méi)有漏入空氣。3、樣氣中氧含量的變化會(huì)受管道材質(zhì)及表面粗糙度影響,因此一般連接管路選用銅管或拋光過(guò)的不銹鋼管,而不用塑料管、橡膠管等。4、微量元素分析時(shí),要避免各種管件、閥門(mén)、表頭等死角對(duì)樣氣造成污染,因此必須盡可能的簡(jiǎn)化氣路系統(tǒng),連接件死角要小,以防止溶解氧逸出造成污染,使用水封、油封及臘封等設(shè)備,才能較好的確保數(shù)據(jù)的。上海禹重實(shí)業(yè)有限公司致力于提供分析儀,...
Procedure–Powder/ChipSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.LoginaminimumofthreeBlankreps.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Inserta***NickelCapsule(leavecapsuleopen)intotheopenportat...
氧氮?dú)浞治鰞x的操作過(guò)程氧氮?dú)浞治鰞x可根據(jù)的用戶的要求定制。該分析儀配備兩個(gè)不同靈敏度的探測(cè)器,在更多的應(yīng)用中保證了準(zhǔn)確度。操作簡(jiǎn)單而且安全。在樣品稱(chēng)重以后,樣品的重量數(shù)據(jù)通過(guò)電子界面?zhèn)鲗?dǎo)至相連的電腦中,也可以在軟件界面中手動(dòng)輸入樣品的重量。樣品被放置在水平放置的爐子中的低溫區(qū)域。分析開(kāi)始以后,爐子開(kāi)始向上轉(zhuǎn)動(dòng),然后樣品逐漸落入加熱區(qū)。通過(guò)添加載體氣體氮?dú)?,氫氣被擴(kuò)散出來(lái)并且隨載體被傳導(dǎo)至一個(gè)高靈敏度的熱傳導(dǎo)測(cè)量池。通常一次測(cè)量的時(shí)間在3到15分鐘之間。在分析的過(guò)程中設(shè)備可以顯示測(cè)試信號(hào)和設(shè)備的參數(shù),從信號(hào)的評(píng)估到結(jié)果在界面上的顯示全部自動(dòng)完成;而測(cè)量數(shù)據(jù)則被傳導(dǎo)至LIMS(實(shí)驗(yàn)室信息管理系統(tǒng))...
Procedure-SolidSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.Loginaminimumof3Blankreplicates.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Placea502-344NickelBasketintotheloadinghead.Note:samplesusinga
ONH836系列:氧氮?dú)浞治鰞x(熔融法)力可ONH836系列儀器采用惰性熔融法,提供各種無(wú)機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金、陶瓷材料中寬范圍的氧氮?dú)渫瑫r(shí)分析。ONH836系列儀器通過(guò)采納客戶的反饋意見(jiàn)和創(chuàng)新設(shè)計(jì),力可儀器采用觸摸屏技術(shù)和在線軟件平臺(tái),增強(qiáng)了儀器的可操作性、降低了分析成本、節(jié)省實(shí)驗(yàn)室桌面空間。用戶友好界面的Cornerstone?軟件力可的Cornerstone氧氮氧分析軟件采用觸摸屏界面使用戶可完整的達(dá)到分析控制、方法設(shè)定、在線診斷、數(shù)據(jù)報(bào)告。Cornerstone氧氮氧分析軟件允許用戶在單一分析界面中完成日常的所有工作,快速而且簡(jiǎn)單易用。力可創(chuàng)新的批次和重復(fù)樣品數(shù)據(jù)分組功能極...
MethodSelectionTwomethodsaredescribedinthisapplicationnote;eithermethodcanbeusedtoanalyzeiron,steel,nickel-,andcobalt-basealloys.ThePrecisionMethodisrecommendedforgeneraluseandwillprovidethebestprecisionandaccuracythroughoutthetypicalO,N,andHconcentrationsfoundinthisgroupofmetals;approximatecycletim
Procedure-SolidSamplesPresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleanerAddapproximately0.05gof***GraphitePowdert
Procedure-SolidSamplesPresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleanerAddapproximately0.05gof***GraphitePowdert
力可OHN736&836系列儀器采用惰性熔融法,提供各種無(wú)機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金陶瓷材料中寬范圍的氧氮?dú)渫瑫r(shí)測(cè)定。ONH836儀器通過(guò)采納客戶的反饋意見(jiàn)和創(chuàng)新設(shè)計(jì),力可儀器采用觸摸屏技術(shù)和在線軟件平臺(tái),增強(qiáng)了儀器的可操作性,降低了分析成本,節(jié)省實(shí)驗(yàn)室桌面空間。用戶友好界面的Cornerstone?軟件力可的Cornerstone碳硫分析軟件采用觸摸屏界面使用戶可完整的達(dá)到分析控制、方法設(shè)定、在線診斷、數(shù)據(jù)報(bào)告。Cornerstone碳硫分析軟件允許用戶在單一分析界面中完成日常的所有工作,快速而且簡(jiǎn)單易用。力可創(chuàng)新的批次和重復(fù)樣品數(shù)據(jù)分組功能極大簡(jiǎn)化了樣品結(jié)果輸出和結(jié)果標(biāo)準(zhǔn)偏差的自動(dòng)計(jì)...
companyprofileShanghaiUzongIndustrialCo.,Ltd.(hereinafterreferredtoasUZONGLAB?)isahigh-techcompanythatprovidesintegratedsolutionsforintelligentlaboratories,mainlyservingtheChinesemarketandcountriesalongthe“BeltandRoad”.IthasthreebusinessdivisionsandoneThetechnologycenter,namelytheinstrumentbusinessd...
ONH836氧氮?dú)浞治鰞x高頻燃燒紅外檢測(cè)技分析無(wú)機(jī)材料中的碳、硫含量。采用惰性氣體保護(hù)熔融法提供各種無(wú)機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金、難熔金屬、陶瓷等材料中寬范圍的氧氮?dú)渫瑫r(shí)分析。該儀器配置MSWindows?的軟件接口,專(zhuān)為觸摸屏操作定制。長(zhǎng)期的開(kāi)發(fā)研究與客戶反饋相結(jié)合,這個(gè)簡(jiǎn)單方便的軟件使得用戶可以快速完整訪問(wèn)儀器控制,分析設(shè)置,故障診斷,數(shù)據(jù)報(bào)告,提高日常分析的效率并節(jié)省用戶寶貴的時(shí)間??蛇x的Cornerstone?Mobile軟件功能,使得用戶可以在手機(jī),便攜式電腦及臺(tái)式電腦上便捷的訪問(wèn)儀器數(shù)據(jù),分析曲線圖形以及儀器的狀態(tài),實(shí)現(xiàn)對(duì)儀器的遙控。上海禹重實(shí)業(yè)有限公司為您提供分析儀,期待您...
氧氮?dú)浞治鰞x是快速、準(zhǔn)確分析氧、氮、氫元素的、高性能儀器,整機(jī)采用模塊化、一體化設(shè)計(jì),即主機(jī)由可靠的脈沖電極爐、高靈敏高精度的檢測(cè)系統(tǒng)、布局合理和氣密性好的氣路系統(tǒng)、可靠耐用的電源系統(tǒng)、穩(wěn)定的電路系統(tǒng)、高校節(jié)能的水循環(huán)散熱系統(tǒng)等六個(gè)**的硬件模塊單元組成。氧氮?dú)浞治鰞x的測(cè)量原理:測(cè)量范圍非常。分析樣品時(shí),樣品被稱(chēng)重后放到樣品端口中,然后用載氣進(jìn)行沖洗,防止大氣(含氧氣和氮?dú)猓┻M(jìn)入到爐子系統(tǒng)中。石墨坩堝在脈沖爐中脫氣,以盡量減少自帶的污染。經(jīng)過(guò)穩(wěn)定階段后樣品落入坩堝中并熔融。樣品中的氧與石墨坩堝中的碳反應(yīng)生成一氧化碳。氮和氫以單質(zhì)的形式釋放。載氣和樣品氣體通過(guò)粉塵過(guò)濾網(wǎng)后再進(jìn)入到氧化銅催化爐中,...
SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsecti
氧氮?dú)浞治鰞x氧氮?dú)浞治鰞x是一種用于材料科學(xué)領(lǐng)域的儀器,于2016年03月09日啟用。技術(shù)指標(biāo)測(cè)量范圍:ON低氧0.0-300ppmOH低氧0.0-300ppm高氧0.0-2%高氧0.0-2%低氮0.0―300ppm低氫0.0-50ppm高氮0.0-2%高氫0.0-1000ppm靈敏度:氧0.01ppm;氮0.1ppm;氫0.01ppm。主要功能該儀器配置有16位微處理器和兩個(gè)的分別檢測(cè)高氧和低氧的紅外檢測(cè)池。氮和氫通過(guò)雙重范圍的熱導(dǎo)檢測(cè)池測(cè)量。分析過(guò)程中可自動(dòng)實(shí)現(xiàn)從低范圍到高范圍的切換。樣品在高功率脈沖爐的石墨坩堝中加熱可達(dá)3000℃以上高溫,脈沖爐采用循環(huán)水冷卻。該儀器具有靈敏度高、性能好、...
companyprofileShanghaiUzongIndustrialCo.,Ltd.(hereinafterreferredtoasUZONGLAB?)isahigh-techcompanythatprovidesintegratedsolutionsforintelligentlaboratories,mainlyservingtheChinesemarketandcountriesalongthe“BeltandRoad”.IthasthreebusinessdivisionsandoneThetechnologycenter,namelytheinstrumentbusinessd...
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.AnalyzeSamples.LoginSamplewiththeappropriatenumberofreps.Weighapproximately***gramsofappropriatelypreparedsampleintoa***NickelCapsule,entermassandsampleidenti...
Procedure-SolidSamplesDeterminetheinstrumentblank.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.Loginaminimumof3Standardreplicates.Weighapproximately***gramsofacalibration/driftstandard,enterth
ONH836氧氮?dú)浞治鰞x高頻燃燒紅外檢測(cè)技分析無(wú)機(jī)材料中的碳、硫含量。采用惰性氣體保護(hù)熔融法,提供各種無(wú)機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金、難熔金屬、陶瓷等材料中寬范圍的氧氮?dú)渫瑫r(shí)分析。該儀器配置MSWindows?的軟件接口,專(zhuān)為觸摸屏操作定制。長(zhǎng)期的開(kāi)發(fā)研究與客戶反饋相結(jié)合,這個(gè)簡(jiǎn)單方便的軟件使得用戶可以快速完整訪問(wèn)儀器控制,分析設(shè)置,故障診斷,數(shù)據(jù)報(bào)告,提高日常分析的效率并節(jié)省用戶寶貴的時(shí)間??蛇x的Cornerstone?Mobile軟件功能,使得用戶可以在手機(jī),便攜式電腦及臺(tái)式電腦上便捷的訪問(wèn)儀器數(shù)據(jù),分析曲線圖形以及儀器的狀態(tài),實(shí)現(xiàn)對(duì)儀器的遙控。上海禹重實(shí)業(yè)有限公司為您提供分析儀,有需...
氧氮?dú)浞治鰞x的優(yōu)點(diǎn)采用惰氣熔融技術(shù),同時(shí)測(cè)定氧、氮和氫元素含量新設(shè)計(jì)封閉氣路系統(tǒng),優(yōu)化氣路循環(huán),使氧氮?dú)錅y(cè)量更準(zhǔn)確可采用更廉價(jià)的氬氣作為載氣催化爐溫度可調(diào),使氧的測(cè)量更加準(zhǔn)確氣路系統(tǒng)都采用電磁閥控制,新增分段式漏氣檢測(cè)水冷樣品加樣端口,有效隔絕雜質(zhì)氣體侵入儀器配置和氧、氮、氫測(cè)量范圍可靈活選擇新設(shè)計(jì)的高靈敏度紅外檢測(cè)池和熱導(dǎo)池,有極低的檢出限分析時(shí)間短脈沖爐功率高達(dá)8.5kw,溫度3000℃顆粒狀樣品無(wú)需膠囊包裹,使用經(jīng)濟(jì)實(shí)惠化學(xué)試劑及管路隱藏在門(mén)后(可移除)強(qiáng)大的分析軟件(支持?jǐn)?shù)據(jù)和應(yīng)用報(bào)告導(dǎo)出、增加評(píng)論區(qū)及其他更多功能)。單點(diǎn)和多點(diǎn)校正(線性回歸)可采用自來(lái)水、冷卻循環(huán)水機(jī)或交換機(jī)冷卻新設(shè)...
氧氮?dú)浞治鰞x的原理:分析樣品在惰性氣流存在下于石墨坩堝中加熱熔融,其中脈沖爐溫度可自由設(shè)定,并通過(guò)一個(gè)非接觸式的光學(xué)溫度傳感器進(jìn)行實(shí)時(shí)監(jiān)控,用于實(shí)現(xiàn)樣品的完全分解,反應(yīng)所生成的COH2和N2被帶入到具有高穩(wěn)定性和靈敏度的檢測(cè)系統(tǒng)進(jìn)行檢測(cè)。對(duì)于CO的檢測(cè)采用的是非色散性紅外檢測(cè)器,對(duì)于N2和H2的檢測(cè)則采用熱導(dǎo)檢測(cè)器。氧氮?dú)浞治鰞x的特點(diǎn):快速準(zhǔn)確分析,自動(dòng)化操作;精密氣體校準(zhǔn);CO紅外檢測(cè)器,高分辨率和重現(xiàn)性的N、H熱導(dǎo)池檢測(cè)器;同一臺(tái)儀器實(shí)現(xiàn)熔融提取和熱提??;熱提取分析時(shí)間可調(diào);可自由選擇溫度高達(dá)2500°C;光學(xué)溫度計(jì)溫度測(cè)定和控制;所有檢測(cè)器自動(dòng)調(diào)零/自動(dòng)水平控制(ALC);數(shù)據(jù)評(píng)估的自動(dòng)...
LECO—YoursourcefortotalanalyticalsolutionsCSCS844and744Series:Carbon/SulfurbyCombustionCarbonandsulfurdeterminationbycombustioninfrareddetectionQuick,accurate,andaffordabledeterminationforbothproductioncontrolandresearchCalibration,analysis,evaluation,anddiagnosticfunctionsaccessibleviauser-friendly...
Oxygen,Nitrogen,andHydrogeninRefractoryMetalsSummaryOneofthemostcriticalchemicalspecificationsoftitaniumalloysisthehydrogencontent.Toohighofahydrogencontentcancausehydridestoprecipitate,whichcanleadtoembrittlementandsubsequentcrackingwhenthealloyisstressed.Hydrogenpickuptypicallyoccursduringdownstre
Procedure–Powder/ChipSamplesDeterminetheinstrumentblank.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodeeithermanuallyorremovethecrucibleandpresstheanalyzebuttontocleanwithanautomaticcleanerifapplicable.Adda...